1 北京工业大学材料与制造学部高功率及超快激光先进制造实验室,北京 100124
2 北京动力机械研究所,北京 100074
飞秒激光以其超窄脉宽和超高光强等特性被广泛应用于各种金属材料的加工。本课题组采用波长为515 nm的绿光飞秒激光器对GH3230镍基高温合金进行刻蚀试验,研究了GH3230高温合金的绿光飞秒激光刻蚀阈值、刻蚀率和极限刻蚀深度。结果表明:相比于红外飞秒激光,绿光飞秒激光的刻蚀阈值明显降低,刻蚀率显著提高;与红外飞秒激光刻蚀类似,随着刻蚀次数增加,刻蚀深度增大,但当刻蚀次数增加到一定值后,刻蚀深度出现饱和现象;激光能量密度越高,极限刻蚀深度越大;改变扫描策略进行双道刻蚀时,通过增加刻缝宽度可以增大刻蚀深度;激光诱导等离子体是影响刻蚀深度的主要因素。
激光技术 镍基高温合金 飞秒激光加工 刻蚀阈值 刻蚀深度 刻蚀率
1 太原理工大学物理与光电工程学院,山西 太原 030024
2 太原理工大学新型传感器与智能控制教育部重点实验室,山西 太原 030024
通过混沌相关光纤环衰荡传感系统实时监测氧化石墨烯沉积过程,并采用氧化石墨烯功能化锥形光纤作为传感元件对血红蛋白传感进行了实验研究。通过实时监测氧化石墨烯对锥形光纤功能化过程中衰荡时间的变化,分析了功能化过程中锥形光纤表面羟基化、硅烷化和氧化石墨烯沉积对光传输损耗的影响。通过扫描电子显微镜对氧化石墨烯功能化锥形光纤效果进行检测。研究了不同浓度的氧化石墨烯功能化锥形光纤作为传感元件时对血红蛋白传感灵敏度的影响,实验结果表明:与未功能化锥形光纤相比,使用氧化石墨烯功能化锥形光纤进行血红蛋白传感,灵敏度提高了一个数量级。在功能化过程中,氧化石墨烯浓度将影响功能化后锥形光纤的传感灵敏度,且随着浓度的增加传感灵敏度增强。该研究成果有望在生物传感领域得到应用。
医用光学与生物技术 锥形光纤 氧化石墨烯 光纤环衰荡 血红蛋白 传感 激光与光电子学进展
2023, 60(5): 0517001
1 浮法玻璃新技术国家重点实验室, 蚌埠 233000
2 硅基材料安徽省实验室, 蚌埠 233000
3 玻璃新材料创新中心(安徽)有限公司, 蚌埠 233000
4 安徽凯盛基础材料科技有限公司, 蚌埠 233000
针对浮法玻璃成形过程, 提出了锡槽入口段简化稳态多相模型, 并采用Ansys Fluent 2019 R3软件, 模拟研究了500 t/d锡槽入口段玻璃液的流动与成形过程, 分析了拉引量、玻璃液黏度对唇砖与八字砖区玻璃液流动与液层厚度分布的影响。结果表明, 拉引量过小或黏度过低时液层出现不连续, 拉引量过大或黏度过高时液层横向厚度均匀性变差, 案例锡槽实现浮法玻璃均匀稳定成形的工艺操作范围是拉引量400~550 t/d, 黏度400~600 Pa·s。
浮法玻璃 锡槽 成形 拉引量 黏度 数值模拟 多相流动 float glass tin bath forming pull rate viscosity numerical simulation multiphase flow
Key Laboratory of Advanced Technologies of Materials (Ministry of Education of China), School of Life Science and Engineering, School of Electrical Engineering, Southwest Jiaotong University, Chengdu 610031, China
采用水热合成法与原位分解法相结合, 在不使用软模板和强碱条件下制备得到了米粒状氧化铜(CuO)。将得到的CuO材料与Nafion溶液混合, 制作成化学修饰电极(CME), 开展葡萄糖的无酶检测。采用X射线衍射仪(XRD)和扫描电子显微镜(SEM)分别对所制备的材料和电极的结构、形貌进行表征、分析。采用线性扫描伏安法、循环伏安法、安培响应和交流阻抗技术对所制备电极进行电化学性能测试。研究结果表明: 所制备的CuO形貌在微观下酷似米粒, 长度为0.5~ 1.0 μm, 直径为250~320 nm。当CuO修饰量为0.35 mg (电极表面积为0.22 cm2)时, 修饰电极对葡萄糖具有较好的电化学检测性能。在0.0357~2.361 mmol/L浓度范围内存在良好的线性关系, 其线性方程为: Ipa(mA)= -0.00187+0.05239c (mmol/L), R2=0.998。检出限为 0.0647 μmol/L, 灵敏度为950.36 μA·L/(mmol·cm2), 且具有良好的选择性和可靠性。
rice-like CuO chemically modified electrode glucose detection 米粒状CuO 化学修饰电极 葡萄糖 检测
Author Affiliations
Abstract
1 School of Control Science and Engineering, Shandong University, Jinan, 250061, China
2 State Key Lab of Microbial Technology, School of Life Science, Shandong University, Jinan, 250100, China
3 School of Materials Science and Engineering, Shandong University, Jinan, 250061, China
A method for detecting protein molecules based on the tilted fiber Bragg grating (TFBG) surface plasma resonance (SPR) is proposed to achieve the quick online real-time detection of trace amount of proteins. The detection principles of the TFBG-SPR protein molecular probe are analyzed, and its feasibility is demonstrated. The intermediary material between the protein molecules and the golden layer outside of the fiber gratings is cysteamine hydrochloride. When the concentration of the cysteamine hydrochloride solution is 2 M, the shift of the TFBG resonance peak is 2.23 nm, illustrating that the cysteamine hydrochloride modifies the gold film successfully. IgG antigen solution is poured on the surface of the cysteamine hydrochloride modifying the gold-deposited TFBG. Finally, antigen-antibody hybridization experiment is carried out with a 10 mg/mL antibody solution, and after two hours of hybridization the resonance peak of the TFBG shifts 5.1 nm, which validates the feasibility and effectiveness of the TFBG-SPR protein molecular probe.
Surface plasma resonance TFBG protein molecular probe Photonic Sensors
2017, 7(4): 317
Author Affiliations
Abstract
School of Control Science and Engineering, Shandong University, Jinan 250061, China
This paper proposes an unprecedented systematic approach for real-time monitoring the temperature and flow of diesel engine by using embedded fiber Bragg grating (FBG). By virtue of FBG’s temperature effect, we design a novel sensitive FBG temperature sensing probe to measure the temperature of cylinder head and inlet flow of diesel engine. We also establish the corresponding software platform for intuitive data analysis. The experimental and complementary simulation results simultaneously demonstrate that the FBG-based optical fiber technique possesses extraordinary reproducibility and sensitivity, which makes it feasible to monitor the temperature and inlet flow of diesel engine. Our work can provide an effective way to evaluate the thermal load of cylinder head in diesel engine.
光电子快报(英文版)
2016, 12(5): 384
桂林电子科技大学 信息与通信学院, 广西 桂林 541004
LDPC(低密度奇偶校验)码常见的编码方法常常无法将校验矩阵的围长和线性无关相统一, 对编译码复杂度和译码性能有一定影响。文章提出了一种低复杂度LDPC的构造方法, 通过构造分块矩阵A和B, 获得一个围长为10、列重为2、具有近似下三角形式的校验矩阵, 且矩阵各行之间线性无关。该码具有以下优点: 较高的围长能提升译码性能; 较低的列重使该码适合在部分响应信道传播; 近似下三角形式和线性无关的特性, 较好地降低了编译码的复杂度。采用Matlab软件的仿真结果表明, 在高斯白噪声信道、BP(置信传播)译码算法下, 该码比普通的10围长LDPC码具有更低的复杂度, 比普通的6围长LDPC码具有更好的译码性能。
低密度奇偶校验码 高围长 低复杂度 近似下三角 线性无关 LDPC code high girth low complexity approximate lower triangular nonsingularity
Author Affiliations
Abstract
1 School of Control Science and Engineering, Shandong University, Jinan, 250061, China
2 State Key Lab of Microbial Technology, School of Life Science, Shandong University, Jinan, 250100, China
In this paper, the response of fiber Bragg gratings (FBGs) subjected to the ultrasonic wave has been theoretically and experimentally investigated. Although FBG sensors have been widely used in the ultrasonic detection for practical structural health monitoring, the relationship between the grating length and ultrasonic frequency is not yet to be obtained. To address this problem, an ultrasound detection system based on FBGs is designed and the response sensitivity of different lengths gratings are detected. Experimental results indicate that the grating with 3 mm length has a higher sensitivity when detecting high frequency ultrasonic wave, and the amplitude can be up to 0.6 mV. The 10 mm length grating has better detection sensitivity for low frequency ultrasonic wave and the amplitude is 0.8 mV. The results of this analysis provide useful tools for high sensitivity ultrasound detection in damage detection systems.
FBG nondestructive testing ultrasonic detection Photonic Sensors
2016, 6(2): 187